Outside cell reaction of indirect electrosynthesis of p-bromobenzoic acid by using Cr2O72-/Cr3+ electrolytic medium in the emulsifying stirrer was studied.
在高剪切混合乳化机搅拌下,采用Cr2O72-/Cr3+作媒质间接电合成对溴苯甲酸槽外反应的优选条件为:原料配比n(Cr2O72-):n(p-Br-C6H4-CH3)=1:3,C(H26O4)=7mol/L,反应温度120℃,反应时间45min,对溴苯甲酸反应收率为81。
Outside cell reaction of indirect electrosynthesis of p-bromobenzoic acid by using Cr_2O_7~(2-)/Cr~(3+) electrolytic medium in the emulsifying stirrer was studied.
在高剪切混合乳化机搅拌下,采用Cr2O72-/Cr3+作媒质间接电合成对溴苯甲酸。
Synthesis and Properties of Complexes of Pr(Ⅲ) and Nb(Ⅲ) with 3-bromobenzoic Acid;
镨(Ⅲ)、钕(Ⅲ)间溴苯甲酸配合物的合成与性质
The solid state complexes of Sc(Ⅲ), Y (Ⅲ), La (Ⅲ), Gd (Ⅲ) with 3-bromobenzoic acid have been synthesized, in order to study their special property.
为考查稀土配合物的特殊性能,合成了间溴苯甲酸与钪(Ⅲ)、钇(Ⅲ)、镧(Ⅲ)、钆(Ⅲ)的四种配合物。
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