The catalytic activity of esterification of diisooctyl terephthalate was studied,with stannous oxide,stannous chloride,stannous octoate and their synergism as catalyst.
以3种亚锡类催化剂氧化亚锡、氯化亚锡、辛酸亚锡以及它们之间复配后作为催化剂,对对苯二甲酸二异辛酯酯化反应的催化活性进行了研究,实验结果表明,以氧化亚锡和辛酸亚锡复配后的催化活性最高,氧化亚锡和辛酸亚锡作为催化剂的酯化反应最佳合成工艺条件为:催化剂的加量为0。
After the sample was dissolved in acidic medium,stannous chloride was used to reduce large parts of trivalent iron into bivalent,under the indication of sodium tungstate,titanium trichloride was used to reduce the remaining trivalent iron into bivalent,and then totassium dichromate was used to oxidize excessive titanium trichloride to eliminate its interference.
试样以盐酸溶解后,在酸性介质中,先以氯化亚锡将三价铁大部分还原为二价,然后在钨酸钠指示下,再以三氯化钛将剩余的三价铁还原为二价,过量的三氯化钛以重铬酸钾氧化消除干扰,在硫磷混合酸存在下,以二苯胺磺酸钠为指示剂,用重铬酸钾标准溶液滴定全铁量。
The flotation behaviors of osmium(Ⅳ) from stannous chloride-cetyltrimetheylammonium bromide-(water) system in the presence of sodium chloride were studied.
研究了氯化钠存在下氯化亚锡-十六烷基三甲基氯化铵体系对Os(Ⅳ)-三氯锡酸络阴离子的浮选行为。